Experiment (E), Report Form and Marking Guide |
Tutorial (T) |
Assessment |
Learning Tools |
References
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Safety notes
Course notes Reagents Table in Excel
Appendix to the manual and the yellow pages
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All homework reports are due at the start of the next E class. In-lab assignments are due at the end of the class in which they have been given. |
Lab
technique tips
Intro to drawing programs
Periodic Table
Molecular
weight calculator |
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E0 Introduction and polyoxomolybdates
Report form for E0 |
T0 Admin & general concepts of spectroscopy.
Answers to practice problems |
T0 In-class workbook
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Video on balancing the equation and stoichiometric ratios
Video on the reagents table and limiting reagent Video on calculating % yield |
Reference 1
Reference 2 |
E1 Chemically active extraction
Report template for E1 |
T1 1H NMR spectroscopy
Answers to practice problems |
E1 pre-lab is on Brightspace
E1Structured report
T1 In-class workbook |
Video on thin layer chromatography
Video on liquid-liquid extraction
Video on using the rotary evaporator
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E2 Electrochemistry of cobalt
Report template for E2
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T2 IR interpretation of infrared spectra
Answers to practice problems
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E2 Structured report
T2 In-class workbook |
Video on balancing the equation and stoichiometric ratios
Video on the reagents table and limiting reagent Video on calculating % yield
Video on
bonding & magnetism Guidelines on balancing redox equations
Standard reduction potentials for common half-reactions
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Reference |
E3 Synthesis and chemistry of alkenes
Report template for E3 |
T3 1H NMR of alkenes and mixtures
Answers to practice problems |
E3 pre-lab is on Brightspace
E3 Structured report
T3 In-class workbook |
Video on setting up a distillation
Review of tlc
Video on using the ATR-IR spectrometer
Video on IR instrumentation
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E4 Thermochromic compounds
Report template for E4
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T4 Titanium structural analysis |
E4 + T4 Structured report and in-lab assignments |
Transition metals, magnetism and colour
Viewing crystal structures
Video on unit cells
Point group determination
Before downloading Mercury (or ChemDraw) you might want to consider using these progams in Ell346. For in-class use, we will provide laptops. The Mercury study will only be for in-class work. |
Reference 1; Reference 2 (just 2 pages needed)
Reference 3;
Extra reference on thermochromism
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E5 Isolation of a natural product
Report template for E5
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T5 13C and DEPT-135 NMR
Answers to practice problems |
E5 pre-lab is on Brightspace
E5 Structured report
T5 In-class workbook |
Video on column chromatography
Review of tlc
Review of rotovaps
Review of ATR-IR |
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E6 Metal acac complexes
Report template for E6
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T6 Metal acac complex IR analysis
IR of acacH as a thin film |
E6 + T6 Structured report |
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E7 Selective reduction
Report template for E7
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T7 Analyses of reduction products |
E7 pre-lab is on Brightspace
E7&T7 Structured report
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Video on NMR instrumentation
Video on NMR sample prep
Review liquid-liquid extraction
Review of rotovaps
Review of ATR-IR
Video on melting ranges |
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E8 Optical activity at an octahedral cobalt centre
Report form for E8 |
T8 Processing NMR spectra |
E8 Report form
T8 In-class workbook |
Video on
inorganic optical isomers
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Reference 1; Reference 2;
Reference 3
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E9 The aldol reaction and an evaluation of sunscreen components
Report template for E9 |
T9 Multinuclear and spin dilute systems in NMR.
Answers to practice problems |
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E10 Sulfur
Report template for E10
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T10 Mass spectrometry
Answers to practice problems |
E10 structured report
T10 In-class workbook |
Video of how a mass spectrometer works |
Reference 1; Reference 2;
Reference 3;
Reference 4 |
E11 The Grignard reaction
Report template for E11 |
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E11 Structured report due at end of class |
Review of ATR-IR
Review melting ranges |
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E12 Tridentate isomerism
Report form for E12
Spectra of isomers |
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E12 Structured report form due at the end of class |
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Reference 1 |
E13 Electrophilic addition - bromination of stilbene
Report form for E13 |
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E14 Triarylphosphine chalcogenides
Report form for E14 |
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Video of how a mass spectrometer works |
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