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Mass Spectrometry of Inorganic and Organometallic Compounds: Tools - Techniques - Tips


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(if you're looking for a quick summary of the techniques we use, I suggest publication 82). Publications 112 and 124 are the first two of a planned series of tutorial reviews that we've chosen to do instead of a second edition of the above text.

Transition Metal Carbonyl Cluster Chemistry

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Journal articles

Links to peer-reviewed journal articles are provided below and numbered 1, 2, 3 etc. Open access articles are indicated by open. Other material (book chapters etc.) are lettered A, B, C etc. More detail on books is available elsewhere.

2020 | 2019 | 2018 | 2017 | 2016 | 2015 | 2014 | 2013 | 2012
2011 | 2010 | 2009 | 2008 | 2007 | 2006 | 2005 | 2004 | 2003 | pre-2003


2020

136. Real-time analysis of methylalumoxane formation
A Joshi, H Zijlstra, E Liles, R Concepcion, M Linnolahti, JS McIndoe*
 Preprint open available at https://doi.org/10.26434/chemrxiv.12830942.v1

136

M. Inexpensive open source laser cut model kits for the teaching of molecular geometry
S Adams, JS McIndoe*
 Preprint open available at https://doi.org/10.26434/chemrxiv.12818780.v1

M

135. Disulfonated xantphos for mass spectrometric mechanistic analysis
M Paul, K Laketic, JS McIndoe*
 Preprint open available at https://doi.org/10.26434/chemrxiv.12797660.v1

135

134. Dynamic ion speciation during hydrolysis of aryltrifluoroborates
I Omari, LPE Yunker, J Penafiel, D Gitaari, A San Roman, JS McIndoe*
 Preprint open available at https://doi.org/10.26434/chemrxiv.12724724.v1

134

133. Trichloro(dinitrogen)platinate(II)
GT Thomas, S Donnecke, I Paci, JS McIndoe*
 Chemistry - A European Journal, in the press
 Preprint open available at https://doi.org/10.26434/chemrxiv.12367472.v1

133

132. Catalyst deactivation processes during 1-hexene polymerization
A Joshi, HS Zijlstra, S Collins, JS McIndoe*
 ACS Catalysis, in the press
 Preprint open available at https://doi.org/10.26434/chemrxiv.12081768.v1

132

131. Real-time monitoring of a cobalt-mediated one-pot transition metal-catalyzed multicomponent reaction
AE Miller-Crotti*, D Previdi, P Donate, JS McIndoe* 
 Inorganica Chimica Acta, in the press
 Preprint open available at https://doi.org/10.26434/chemrxiv.11959128.v1

131

130. Gas-phase oxidation of reactive organometallic ions
A Joshi, S Donnecke, O Granot, D Shin, S Collins, I Paci and JS McIndoe*
 Dalton Transactions, in the press
 Preprint open available at https://doi.org/10.26434/chemrxiv.11909397.v1

130

129. Magnesium-accelerated Maillard reactions drive differences in adjunct and all-malt brewing
IO Omari, HM Charnock, AL Fugina, EL Thomson* and JS McIndoe*
 Journal of the American Society of Brewing Chemists, in the press
 Preprint open available at https://doi.org/10.26434/chemrxiv.10257686.v1

129

128. Orbital shaped standing waves using Chladni plates
E Janusson, J Penafiel, S MacLean, A Macdonald, I Paci* and JS McIndoe*
 Preprint open available at https://doi.org/10.26434/chemrxiv.10255838.v1
 The Chemical Educator, in the press

128

127. Experimental strategies for avoiding saturation effects in ESI-MS
AAJ Wei, A Joshi, Y Chen and JS McIndoe*
 Preprint open available at https://doi.org/10.26434/chemrxiv.8872487.v1
 International Journal of Mass Spectrometry, in the press

127


2019

126. Step-by-step real time monitoring of a catalytic amination reaction
GT Thomas, E Janusson, HS Zijlstra and JS McIndoe*
 Chemical Communications, 2019, 55, 11727-11730 (1.9 MB Download a pdf file of this article file)
 Preprint open available at https://doi.org/10.26434/chemrxiv.8345594.v1

126

125. An information-rich graphical representation of catalytic cycles
J McFarlane, B Henderson, S Donnecke and JS McIndoe*
An editorial in Organometallics, 2019, 38, 4051-4053 (2 MB Download a pdf file of this article file)
 Preprint open available at https://doi.org/10.26434/chemrxiv.8206637.v1
 Try out this tool right now at catacycle.com
 Updated in 2020 to remove limit on number of steps and to add functionality for a second cycle

125

124. Assigning the ESI mass spectra of organometallic compounds
KL Vikse* and JS McIndoe*
 Journal of Mass Spectrometry, 2019, 54, 466-479 (1.2 MB Download a pdf file of this article file)
 Tutorial review; feature article and cover for May 2019

124

123. Interaction of neutral donors with methylaluminoxane
H Zijlstra, A Joshi, M Linnolahti, S Collins, JS McIndoe*
 European Journal of Inorganic Chemistry, 2019, 2346-2355 (VIP status) (1.8 MB Download a pdf file of this article file)
  Interview with editor available at bit.ly/2VMAmUp
  Preprint open available at https://doi.org/10.26434/chemrxiv.7701710.v1

123

122. Structure, anion, and solvent effects on cation response in ESI-MS
I Omari, P Randhawa, J Randhawa, J Yu, JS McIndoe*
  Journal of the American Society for Mass Spectrometry, 2019, 30, 1750-1757 (1.2 MB Download a pdf file of this article file)
  Preprint open available at https://doi.org/10.26434/chemrxiv.7723226.v1

122

121. Confounding contaminants in mass spectrometric reaction monitoring
GT Thomas, L MacGillvray, NL Dean, RL Stoddard, LPE Yunker, JS McIndoe*
  International Journal of Mass Spectrometry, 2019, 441, 14-18 (1 MB Download a pdf file of this article file)
  Preprint open available at https://doi.org/10.26434/chemrxiv.7488737

121

120. PythoMS: A Python framework to simplify and assist in the processing and interpretation of mass spectrometric data
LPE Yunker*, S Donnecke, M Ting, D Yeung, JS McIndoe*
  Journal of Chemical Information and Modeling, 2019, 59, 1295-1300 (1.2 MB Download a pdf file of this article file)
 Tutorial videos available: Windows installation, conversion of RAW files to mzML, isotope pattern overlay, Pyrsir, video renderer script in Windows or Mac.
  Preprint open available at https://doi.org/10.26434/chemrxiv.7264175

120


2018

119. Modifying methylalumoxane via alkyl exchange
HS Zijlstra, A Joshi, M Linnolahti, S Collins, JS McIndoe*
  Dalton Transactions, 2018, 47, 17291-17298 (1.5 MB Download a pdf file of this article file)
  Part of the themed web collection "Inorganic Chemistry of the p-Block Elements"
  Preprint open available at https://doi.org/10.26434/chemrxiv.7243472

119

118. Competitive Ligand Exchange and Dissociation in Ru Indenyl Complexes
RG Belli, Y Wu, H Ji, A Joshi, LPE Yunker, L Rosenberg*, JS McIndoe*    These authors contributed equally
  Inorganic Chemistry, 2019, 58, 747-755 (2.9 MB Download a pdf file of this article file)
  Preprint open available at https://doi.org/10.26434/chemrxiv.7215320

118

118

117. Real-time mass spectrometric investigations into the mechanism of the Suzuki-Miyaura reaction
LPE Yunker, Z Ahmadi, JR Logan, W Wu, T Li, A Martindale, AG Oliver and JS McIndoe*
Organometallics, 2018, 37, 4297-4308 (2.9 MB Download a pdf file of this article file)

117

116. Acid-selective mass spectrometric analysis of petroleum fractions
I Omari, H Zhu, GB McGarvey, JS McIndoe*
  International Journal of Mass Spectrometry, 2019, 435, 315-320 (1.0 MB Download a pdf file of this article file)

113

115. Synthesis, characterization and mass spectrometric analysis of [LSn(VI)F4-x]x+ salts [L = tris((1-ethylbenzoimidazol- 2-yl)methyl)amine, x = 1-4]
R Suter, A Swidan, H Zijlstra, C Macdonald, JS McIndoe and N Burford*
Dalton Transactions, 2018, 47, 16729-16736 (1.5 MB Download a pdf file of this article file)

115

114. Open source laser cut model kits for the teaching of molecular geometry
NL Dean, C Ewan, D Braden and JS McIndoe*
  Journal of Chemical Education, 2019, 96, 495-499 (2 MB Download a pdf file of this article file)
  Files for downloading: individualparts.dxf, T.stl, bent120.stl, bent109.stl, single180.stl, single109.stl. Please email Scott for the (very large!) nested cutting files if you do not have access to the SI of the paper.

114
114

113. Oxidation of methylalumoxane oligomers: A theoretical study guided by mass spectrometry
E Endres, HS Zijlstra, S Collins, JS McIndoe, M Linnolahti*
  Organometallics, 2018, 37, 3936-3942 (2.7 MB Download a pdf file of this article file)

113

112. Ionization methods for the mass spectrometry of organometallic compounds
K Vikse* and JS McIndoe*
  Journal of Mass Spectrometry, 2018, 53, 1026-1034 (837 kB Download a pdf file of this article file)
  Tutorial review; feature article and cover for October 2018

112

111. Fluoride-mediated Exchange of Phenylfluorosilanes
NL Dean, JS McIndoe*
  Canadian Journal of Chemistry, 2018, 96, 587-590 (710 kB Download a pdf file of this article file)

111

110. Oxidation of Methylalumoxane Oligomers
HS Zijlstra, S Collins, JS McIndoe*
  Chemistry - A European Journal, 2018, 24, 5506-5512 (1.9 MB Download a pdf file of this article file)
  Cover image:

110

109. (Ge2P2)2-: a binary analogue of P4 as a precursor to the ternary cluster anion [Cd3(Ge3P)3]3-
S Mitzinger, J Bandemehr, K Reiter, JS McIndoe, X Xie, F Weigend, JF Corrigan, S Dehnen*
  Chemical Communications, 2018, 54, 1421-1424 (3.1 MB Download a pdf file of this article file)

109


2017

108. Oxidation of Titanocene(III): The Deceptive Simplicity of a Color Change
D Yeung, J Penafiel, HS Zijlstra, JS McIndoe*
  Inorganic Chemistry, 2018, 57, 457-461 (1.4 MB Download a pdf file of this article file)

108

107. Phenol-selective mass spectrometric analysis of petroleum fractions
H Zhu, E Janusson, J Luo, J Piers, F Islam, GB McGarvey, AG Oliver, O Granot, JS McIndoe*
  The Analyst, 2017, 142, 3278-3284 (1.2 MB Download a pdf file of this article file)

107

106. Mass transfer and convection effects in small-scale catalytic hydrogenation
J Luo, Y Wu, HS Zijlstra, DA Harrington*, JS McIndoe*
  Catalysis Science and Technology, 2017, 7, 2609-2615 (2.9 MB Download a pdf file of this article file)
  HOT article for 2017

106

105. Additive and Aging Effects on Methylalumoxane Oligomers
HS Zijlstra, M Linnolahti, S Collins, JS McIndoe*
  Organometallics, 2017, 36, 1803-1809 (2.5 MB Download a pdf file of this article file)

105

104. Real-Time Analysis of Pd2(dba)3 Activation by Phosphine Ligands
E Janusson, HS Zijlstra, PPT Nguyen, L MacGillivray, J Martelino, JS McIndoe*
  Chemical Communications, 2017, 53, 854-856 (1.9 MB Download a pdf file of this article file)

103

 


2016

103. Electron ionization mass spectrometric analysis of air- and moisture-sensitive organometallic compounds
J Penafiel, AV Hesketh, O Granot*, JS McIndoe*
  Dalton Transactions, 2016, 45, 15552-15556 (1.4 MB Download a pdf file of this article file)

103

102. Applying handheld 3D printing technology to the teaching of VSEPR theory
N Dean, C Ewan, JS McIndoe*
  Journal of Chemical Education, 2016, 93, 1660-1662 (2 MB Download a pdf file of this article file)

100

101. Alkylation of [Pt2(µ-S)2(PPh3)4] with boronic acid derivatives
OT Ujam*, OE Offie, PO Ukoha, AG Oliver, JI Ume, RL Stoddard, JS Mclndoe
  Journal of Coordination Chemistry, 2016, 49, 2807-2818

102

100. Simultaneous orthogonal methods for the real-time analysis of catalytic reactions
R Theron, Y Wu, LPE Yunker, AV Hesketh, I Pernik, AS Weller, JS McIndoe*
  ACS Catalysis, 2016, 6, 6911-6917 (1.6 MB Download a pdf file of this article file)

100

99. Selective mass spectrometric analysis of thiols using charge-tagged disulfides
E Janusson, GB McGarvey, F Islam, C Rowan, JS McIndoe*
  Analyst, 2016, 141, 5520-5526 (700 kB Download a pdf file of this article file)

99

98. Mass spectrometric characterization of oligomeric phosphaalkenes
BT Gillon, DP Gates*, MA Henderson, E Janusson, JS McIndoe*
  Canadian Journal of Chemistry, in the press (1.2 MB Download a pdf file of this article file)

98

97. Reactivity of [Pt2(µ-S)(PPh3)4] towards activated aliphatic bromoacyl electrophiles: formation of mono-, homodi-, heterodi- and intramolecular-bridged dialkylated products
OT Ujam*, E Janusson, RL Stoddard, JS Mclndoe, AG Oliver, PC Odo, OC Ogbonna
  Inorganica Chimica Acta, 2016, 450, 92-100 (1.1 MB Download a pdf file of this article file)

97

L. Mass Spectrometry of Organoaluminum Derivatives
RL Stoddard, S Collins and JS McIndoe*
 Chapter in Patai's Chemistry of Functional Groups. 1–15, ed. I. Marek. John Wiley & Sons, Ltd: Chichester, UK (2016) (716 kB Download a pdf file of this article file)

L
96. Bond Fission in Monocationic Frameworks: Diverse Fragmentation Pathways for Phosphinophosphonium Cations
KL Bamford, SS Chitnis, RL Stoddard, JS McIndoe* and N Burford*
  Chemical Science, 2016, 7, 2544-2552 (1.4 MB Download a pdf file of this article file)
96

2015

95. Mechanistic features of the copper-free Sonogashira reaction from ESI-MS
Z Ahmadi, LPE Yunker, AG Oliver and JS McIndoe*
 Dalton Transactions, 2015, 44, 20367-20375 (1.8 MB Download a pdf file of this article file)

95

94. Reversible Mechanical Interlocking of D-Shaped Molecular Karabiners bearing Coordination-Bond Loaded Gates: Route to Self-Assembled [2]Catenanes
S Prusty, S Krishnaswamy, S Bandi, B Chandrika, J Luo, JS McIndoe, GS Hanan and DK Chand*
 Chemistry - A European Journal, 2015, 21, 15174–15187 (4.4 MB Download a pdf file of this article file)

94

93. Simplified real time mass spectrometric analysis of reactions
AV Hesketh, S Nowicki, K Baxter, RL Stoddard and JS McIndoe*
 Organometallics, 2015, 34, 3816-3819 (1.4 MB Download a pdf file of this article file)

93

92. Spatial effects on electrospray ionization response
E Janusson, A Hesketh, K Bamford, K Hatlelid, R Higgins and JS McIndoe*
 International Journal of Mass Spectrometry, 2015, 388, 1–8 (1.5 MB Download a pdf file of this article file)

92

91. Rhodium-catalyzed selective partial hydrogenation of alkynes
J Luo, R Theron, LJ Sewell, TN Hooper, AS Weller, AG Oliver and JS McIndoe*
 Organometallics, 2015, 34, 3021-3028 (1.5 MB Download a pdf file of this article file)

91

90. Mechanistic insights from mass spectrometry: examination of the elementary steps of catalytic reactions in the gas phase
KL Vikse* and JS McIndoe*
Pure and Applied Chemistry, 2015, 87, 361-377 (4.1 MB Download a pdf file of this article file)
 Invited paper based on ICPOC22 presentation.

91

89. Mass spectrometric characterization of methylaluminoxane-activated, metallocene complexes
TK Trefz, MA Henderson, M Linnolahti, S Collins* and JS McIndoe*
 Chemistry - A European Journal, 2015, 21, 2980-2991 (895 kB Download a pdf file of this article file)

89

2014

88. Solvent effects on surface activity of aggregate ions in electrospray ionization
J Pape, KL Vikse, E Janusson, N Taylor and JS McIndoe*
 International Journal of Mass Spectrometry, 2014, 373, 66-71 (337 kB Download a pdf file of this article file)

85

87. Relative binding affinities of fluorobenzene ligands in cationic rhodium bisphosphine fluorobenzene complexes probed using collision-induced dissociation
SD Pike*, I Pernik, R Theron, JS McIndoe* and AS Weller*
 open Journal of Organometallic Chemistry, 2015, 784, 75-83 (1.4 MB Download a pdf file of this article file)

85

86. A multi-pronged mechanistic study of the phosphine-mediated conjugate addition of an alcohol to an acetylenic ester
RL Stoddard, J Luo, N van der Wal, NF O'Rourke, JE Wulff* and JS McIndoe*
 open New Journal of Chemistry, 2014, 38, 5382-5390 (2.8 MB Download a pdf file of this article file)

85

85. The application of electrospray ionization mass spectrometry to homogeneous catalysis
K Vikse, Z Ahmadi, JS McIndoe*
 Coordination Chemistry Reviews, 2014, 279, 96-114 (5.65 MB Download a pdf file of this article file)

85

84. Exploring the mechanism of the hydroboration of alkenes by amine–boranes catalysed by [Rh(xantphos)]+
HC Johnson, R Torry-Harris, L Ortega, R Theron, JS McIndoe, AS Weller*
 open Catalysis Science &Technology, 2014, 4, 3486-3494 (1.13 MB Download a pdf file of this article file)

84

83.  Electrostatic and non-covalent interactions in dicationic imidazolium-sulfonium salts with mixed anions
Z Fei, D-R Zhu, N Yan, X Yang, TJ Geldbach, R Scopelliti, S Katsuba, G Laurenczy, DM Chisholm, JS McIndoe*, KR Seddon, PJ Dyson*
 Chemistry - A European Journal, 2014, 20, 4273-4283 (1.36 MB Download a pdf file of this article file).

83

82.  Practical approaches to the ESI-MS analysis of catalytic reactions
LPE Yunker, RL Stoddard, JS McIndoe*
 Journal of Mass Spectrometry, 2014, 49, 1-8 (635 kB Download a pdf file of this article file)
 Special Feature Article, journal cover.

82

2013

81.  A mechanistic investigation of hydrodehalogenation using ESI-MS
Z Ahmadi, JS McIndoe*
 open Chemical Communications, 2013, 49, 11488-11490 (1.39 MB Download a pdf file of this article file).

81

80.  Oxidative additions of aryl halides to palladium proceed through the mono-ligated complex
K Vikse, T Naka, JS McIndoe*, M Besora and F Maseras*
 ChemCatChem, 2013, 5, 3604-3609 (182 kB Download a pdf file of this article file).

80

79.  A detailed kinetic analysis of rhodium-catalyzed alkyne hydrogenation
J Luo, AG Oliver and JS McIndoe*
 open Dalton Transactions, 2013, 42, 11312-11318 (1.2 MB Download a pdf file of this article file).
 Recommended by the referees as a "Hot Paper".

79

78.  Gas phase reactivity of iron pentacarbonyl with anionic metal clusters
MA Henderson and JS McIndoe*
 International Journal of Mass Spectrometry, 2013, 354-355, 257-262 (1.14 MB Download a pdf file of this article file).
 Detlef Schröder Memorial Issue

78

77.  Mass spectrometric characterization of methylaluminoxane
T Trefz, MA Henderson, M Wang, S Collins* and JS McIndoe*
 Organometallics, 2013, 32, 3149-3152 (576 kB Download a pdf file of this article file).

77

76.  An unexpected pathway for ligand substitution in an aryl halide complex of palladium
Z Ahmadi, AG Oliver and JS McIndoe*
 ChemPlusChem, 2013, 78, 632-635 (774 kB Download a pdf file of this article file).

76

75.   Synthesis and characterization of a new class of anti-angiogenic agents based on ruthenium clusters
AA Nazarov, M Baquié, P Nowak-Sliwinska, O Zava, JR van Beijnum, M Groessl, DM Chisholm, Z Ahmadi, JS McIndoe, AW Griffioen, H van den Bergh and PJ Dyson
 Scientific Reports, 2013, 3, 1485 (open access).

75

74.  Characterization of isobutylaluminoxanes by electrospray ionization mass spectrometry
MA Henderson, T Trefz, S Collins, M Wang and JS McIndoe*
 Organometallics, 2013, 32, 2079-2083 (544 kB Download a pdf file of this article file).

74

73.  Fixed charge phosphine ligands to explore gas-phase coinage metal mediated decarboxylation reactions
K Vikse, GN Khairallah, JS McIndoe and RAJ O'Hair
 Dalton Transactions, 2013, 42, 6440-6449 (988 kB Download a pdf file of this article file).

73

72.  The color-changing sports drink: an ingestible demonstration
R Stoddard and JS McIndoe
 Journal of Chemical Education, 2013, 90, 1032-1034 (1.1 MB Download a pdf file of this article file).

72

71.  Mass spectrometric transmutation of fullerenes
W Henderson and JS McIndoe*
 Fullerenes, Nanotubes and Carbon Nanostructures, 2014, 22, 663-669 (5.19 MB Download a pdf file of this article file).

71

2012

70. 1,8-bis(dimethylamino)-2-(4-methoxyphenyl)naphthalene: An effective electrospray-active analogue for eta-6-coordinating ligands
KL Vikse, S Kwok, R McDonald, AG Oliver and JS McIndoe*
 Journal of Organometallic Chemistry, 2012, 716, 252-257 (717 kB Download a pdf file of this article file).

70

69. Pressurized sample infusion: an easily calibrated, low volume pumping system for ESI-MS analysis
KL Vikse, Z Ahmadi, J Luo, N van der Wal, K Daze, N Taylor and JS McIndoe*
 International Journal of Mass Spectrometry, 2012, 323-324, 8-13 (763 kB Download a pdf file of this article file).

68. Proton sponge phosphanes: reversibly chargeable ligands for ESI-MS analysis
NJ Farrer, KL Vikse, R McDonald and JS McIndoe*
 European Journal of Inorganic Chemistry, 2012, 733-740 (654 kB Download a pdf file of this article file).

68


2011

67. The Pauson-Khand reaction: a gas phase and solution phase examination using electrospray ionization mass spectrometry
MA Henderson, J Luo, AG Oliver and JS McIndoe*
 Organometallics, 2011, 30, 5471–5479 (2.4 Mb Download a pdf file of this article file).

67

66. A mass spectrometric and theoretical study of polyiodides: the connection between solid state, solution and gas phases
M Groessl, Z Fei, PJ Dyson*, SA Katsyuba*, KL Vikse and JS McIndoe*
 Inorganic Chemistry, 2011, 50, 9728-9733 (2.7 Mb Download a pdf file of this article file).
 Highlighted on ACS's Noteworthy Chemistry, Jan 16 2012.

66

65. Powerful insight into catalytic mechanisms through simultaneous monitoring of reactant, products and intermediates
KL Vikse, Z Ahmadi, CC Manning, DA Harrington and JS McIndoe*
 Angewandte Chemie, International Edition, 2011, 50, 8304-8306 (640 kb Download a pdf file of this article file).
 Selected by the editors as a "Hot Paper".

65

64. Blurring the line between solution and the gas phase: evaporation of water from hypersolvated lanthanide trications provides insights into solution acidity
JL Pape, K McQuinn, F Hof and JS McIndoe*
 New Journal of Chemistry, 2011, 35, 1582-1587 (4 Mb Download a pdf file of this article file).
 The art below was selected for the outside front cover image for the August edition.

njc

63. 3,3’ N,N’ bis(amino) 2,2’ bipyridine: an unusually methylation-resistant amine
DM Chisholm, RM McDonald and JS McIndoe*
 Canadian Journal of Chemistry, 2011, 89, 971-977 (233 kb Download a pdf file of this article file)

62. Using NMR and ESI-MS to Probe the Mechanism of Silane Dehydrocoupling Catalyzed by Wilkinson's Catalyst
SL Jackson, DM Chisholm, JS McIndoe* and L Rosenberg*
 European Journal of Inorganic Chemistry, 2011, 327-330 (363 kb Download a pdf file of this article file).


2010

61. Pressurized sample infusion for the continuous analysis of air- and moisture-sensitive reactions using electrospray ionization mass spectrometry
KL Vikse, MP Woods and JS McIndoe*
 Organometallics, 2010, 29, 6615-6618 (2028 kb Download a pdf file of this article file).

60. 1,3,5-Triazaadamantan-7-amine
J Thomson, DM Chisholm, AG Oliver* and JS McIndoe*
 Acta Cryst., 2010, E66, o2637 (266 kb Download a pdf file of this article file).

59. Direct observation of key intermediates by negative-ion electrospray ionisation mass spectrometry in palladium-catalysed cross-coupling
KL Vikse, MA Henderson, AG Oliver and JS McIndoe*
 Chemical Communications, 2010, 46, 7412-7414 (666 kb Download a pdf file of this article file).

K. Mass spectrometry in organometallic chemistry
JS McIndoe
a chapter in the book Spectroscopic Properties of Inorganic and Organometallic Compounds: pages 288-309 (812 kb Download a pdf file of this article file, preprint)
Edited by J Yarwood, R Douthwaite and SB Duckett
RSC Publishing: Cambridge, 2010.

J. Book Review of Mass Spectrometry and Gas-Phase Chemistry of Non-Covalent Complexes
JS McIndoe
Angewandte Chemie, Internation Edition, 2010, 49, 3717 (233 kb Download a pdf file of this article file).

I. Ionic liquids: solutions for electrospray ionization mass spectrometry
MA Henderson, JS McIndoe and PJ Dyson
a chapter in the book Ionic Liquids: From Knowledge to Application: pages 135-146 (233 kb Download a pdf file of this article file, preprint)
Edited by NV Plechkova, RD Rogers and KR Seddon
American Chemical Society: Washington, 2010.

58. Mono-alkylated bisphosphines as dopants for ESI-MS analysis of catalytic reactions
DM Chisholm, AG Oliver and JS McIndoe*
 Dalton Transactions, 2010, 39, 364-373 (552 kb Download a pdf file of this article file).
 Special Issue: New Talent.
 Selected as a "Hot Paper" (screenshot).


2009

57. Distannoxane speciation during esterification catalysis: revealing insights provided by electrospray ionization mass spectrometry
E Crawford, T Lohr, EM Leitao, S Kwok and JS McIndoe*
 Dalton Transactions, 2009, 9110-9112 (166 kb Download a pdf file of this article file).
 Selected as a "Hot Paper" (screenshot).

56. Bisphosphine monoxides with o-phenylene backbones in Pt, Pd and Fe complexes
NJ Farrer, R McDonald, T Piga and JS McIndoe*
 Polyhedron, 2010, 29, 254-261 (452 kb Download a pdf file of this article file).
 Special Issue: "Polyhedron - The Next Generation"

55. Evidence of asymmetric cation solvation from the instability of [Pb(H2O)n]2+ complexes
K McQuinn, F Hof*, JS McIndoe*, X Chen, G Wu and AJ Stace*
 Chemical Communications, 2009, 4088-4090 (1001 kb Download a pdf file of this article file).

54. Gas-phase reactivity of ruthenium carbonyl cluster anions
MA Henderson, S Kwok and JS McIndoe*
 Journal of the American Society of Mass Spectrometry, 2009, 20, 658-666 (1088 kb Download a pdf file of this article file).

53. Collision-induced dissociation of protonated nanodroplets
K McQuinn, F Hof* and JS McIndoe*
 International Journal of Mass Spectrometry, 2009, 279, 32-36 (467 kb Download a pdf file of this article file).


2008

52. Coupling an electrospray ionization mass spectrometer with a glove box: a straightforward, powerful and convenient combination for analysis of air-sensitive organometallics
AT Lubben, JS McIndoe* and AS Weller*
 Organometallics, 2008, 27, 3303-3306 (91 kb Download a pdf file of this article file).

51. Charged ligands for catalyst immobilisation and analysis
DM Chisholm and JS McIndoe*
 Dalton Transactions, 2008, 3933-3945 (708 kb Download a pdf file of this article file).

50. Insights into post-translational methylation of arginine from studies of guanidinium-water nanodroplets
K McQuinn, JS McIndoe* and F Hof*
 Chemistry - A European Journal, 2008, 14, 6483-6489 (373 kb Download a pdf file of this article file).

49. (Chloromethyl)pentacarbonylmanganese(I); a crystal structure with a non-crystallographic centre of symmetry
BK Nicholson*, JS McIndoe, DA Clementec and WT Robinson
 Structural Chemistry, 2008, 19, 489-492 (187 kb Download a pdf file of this article file).

H. Book Review of Inorganic Mass Spectrometry: Principles and Applications
JS McIndoe
Journal of the American Chemical Society, 2008, 130, 8566-8577 (74 kb Download a pdf file of this article file).


2007

48. Direct observation of ion evaporation from a triply charged nanodroplet
K McQuinn, F Hof* and JS McIndoe*
 Chemical Communications, 2007, 4099-4101 (415 kb Download a pdf file of this article file).
 Selected as a "Hot Paper".

47. Reversible binding of dihydrogen in multimetallic complexes
AS Weller* and JS McIndoe*
 European Journal of Inorganic Chemistry, 2007, 4411-4423 (368 kb Download a pdf file of this article file).

46. Investigation into the formation of heteronuclear clusters of formula [{Ru6C(CO)16Ag2X}2]2– (X = Cl, Br or I)
DM Chisholm, JS McIndoe*, G Bodizs, WH Ang, R Scopelliti and PJ Dyson*
 Journal of Cluster Science, 2007, 18, 303-318 (807 kb Download a pdf file of this article file).

45. Sequential reduction of high hydride count rhodium octahedral clusters [Rh6(PR3)6H12][BArF4]2: redox-switchable hydrogen storage
SK Brayshaw, A Harrison, JS McIndoe, F Marken, PR Raithby, JE Warren and AS Weller*
 Journal of the American Chemical Society, 2007, 129, 1793-1804 (593 kb Download a pdf file of this article file).

G. Metal Carbonyls
JS McIndoe and PJ Dyson
Encyclopedia of Chemical Technology, Concise, 5th Edition (84 kb Download a pdf file of this article file).
John Wiley & Sons Publishers, 2007.

F. Energy-dependent electrospray ionization mass spectrometry
JS McIndoe
a chapter in the Encyclopedia of Mass Spectrometry, Volume 6: pages 467-474 (320 kb Download a pdf file of this article file, preprint).
Elsevier Publishers, 2007.

E. Mass spectrometry of organometallic compounds
NJ Farrer and JS McIndoe
a chapter in the Encyclopedia of Mass Spectrometry, Volume 6: pages 903-915 (249 kb Download a pdf file of this article file, preprint).
Elsevier Publishers, 2007.


2006

44. The energetics of the X2 + X → X3 equilibrium (X = Cl, Br, I) in aqueous and non-aqueous solution
E Crawford, JS McIndoe* and DG Tuck
 Canadian Journal of Chemistry, 2006, 84, 1607-1613 (136 kb Download a pdf file of this article file).

43. Proton sponge phosphines: electrospray-active ligands
NJ Farrer, R McDonald and JS McIndoe*
 Dalton Transactions, 2006, 4570 - 4579 (331 kb Download a pdf file of this article file).
 Selected as a "Hot Paper".
 Featured in Chemical Science, "Victoria proton sponge rises to catalytic challenge".

42. Ionic liquids enable electrospray ionisation mass spectrometry in hexane
MA Henderson and JS McIndoe*
 Chemical Communications, 2006, 2872-2874 (403 kb Download a pdf file of this article file).
 Selected as a "Hot Paper".
 Featured in Chemical Technology, "Broadening the mass spectrum".

41. Storing and Releasing Hydrogen with a Redox Switch
SK Brayshaw, JC Green, N Hazari, JS McIndoe, F Marken, PR Raithby and AS Weller*
 Angewandte Chemie International Edition, 2006, 45, 6005-6008 (221 kb Download a pdf file of this article file).
 Selected as a "Hot Paper".
 Featured as a "Research Highlight" in Nature.
 Highlighted in Green Chemistry.

40. High hydride count rhodium octahedra, [Rh6(PR3)6H12][BArF4]2 : synthesis, structures and reversible hydrogen uptake under mild conditions
SK Brayshaw, M Ingleson, JC Green, JS McIndoe, PR Raithby, G Kociok-Köhn and AS Weller*
 Journal of the American Chemical Society, 2006, 128, 6247-6263 (896 kb Download a pdf file of this article file).

39. Energy dependent electrospray ionisation mass spectrometry of carbonyl clusters
E Crawford, PJ Dyson, O Forest, S Kwok and JS McIndoe*
Journal of Cluster Science, 2006, 17, 47-63 (453 kb Download a pdf file of this article file).
 Invited article for the BFG Johnson retirement issue.

D. Trinuclear Ru / Os clusters containing arene ligands
PJ Dyson and JS McIndoe
Comprehensive Organometallic Chemistry 3
 Elsevier Publishers, 2006.


2005

BK2.  Mass Spectrometry of Inorganic and Organometallic Compounds: Tools - Techniques - Tips 
William Henderson and J. Scott McIndoe
 Part of "Inorganic Chemistry: A Textbook Series"
 John Wiley & Sons Publishers, 2005.
 More details here.

book2

38. Holding onto lots of hydrogen: a 12-hydride-rhodium cluster that reversibly adds two molecules of H2
SK Brayshaw, M Ingleson, JC Green, PR Raithby, G Kociok-Köhn, JS McIndoe and AS Weller*
 Angewandte Chemie International Edition, 2005, 44, 6875-6878 (176 kb Download a pdf file of this article file).
 Selected as a "Hot Paper".

37. Hydrogen sponge? A heteronuclear cluster that absorbs large quantities of hydrogen
PJ Dyson and JS McIndoe
 Angewandte Chemie International Edition, 2005, 44, 5772-5774 (139 kb Download a pdf file of this article file).

36. EDit: a computer program to assist in the presentation of energy-dependent mass spectra
SLG Husheer, O Forest, M Henderson and JS McIndoe*
 Rapid Communications in Mass Spectrometry, 2005, 19, 1352-1354 (307 kb Download a pdf file of this article file).
 Webpage for program download and supporting information.


2004

35. An octahedral rhodium cluster with six phosphine and 12 hydride ligands and 10 too few electrons
PJ Dyson and JS McIndoe
 Angewandte Chemie International Edition, 2004, 43, 6028-6030 (805 kb Download a pdf file of this article file).

34. Direct probe electrospray (and nanospray) ionization mass spectrometry of neat ionic liquids
PJ Dyson,* I Khalaila, S Luettgen, JS McIndoe* and D Zhao
 Chemical Communications, 2004, 2204-2205 (310 kb Download a pdf file of this article file).

33. Analysis of low oxidation state transition metal clusters by laser desorption/ionisation time-of-flight mass spectrometry
PJ Dyson,* AK Hearley, BFG Johnson,* PRR Langridge-Smith and JS McIndoe*
 Inorganic Chemistry, 2004, 43, 4962-4973 (276 kb Download a pdf file of this article file).

32. On the catalytic activity of cluster anions in styrene hydrogenation: considerable enhancements in ionic liquids compared to molecular solvents
PJ Dyson*, G. Laurenczy, JS McIndoe and D Zhao
 Journal of Molecular Catalysis A: Chemical, 2004, 214, 19-25 (129 kb Download a pdf file of this article file).


2003

31. Analysis of coordination and organometallic compounds using photo-ionisation mass spectrometric techniques
A Dorcier, PJ Dyson* and JS McIndoe
 European Journal of Inorganic Chemistry, 2003, 4294-4297 (98 kb Download a pdf file of this article file).

30. A strategy for generating naked metal clusters for gas-phase reactivity studies by FTICR-MS
CPG Butcher, A Dinca, PJ Dyson, BFG Johnson, PRR Langridge-Smith and JS McIndoe*
 Angewandte Chemie, International Edition, 2003, 42, 5752-5755 (1514 kb Download a pdf file of this article file).
 Angewandte Chemie, 2003, 115, 5930-5933.

29. Analysis of organometallic compounds using ion trap mass spectrometry
PJ Dyson and JS McIndoe
 Inorganica Chimica Acta, 2003, 354, 68-74 (704 kb Download a pdf file of this article file).
 Invited article for "Protagonists in chemistry: BFG Johnson" edition.
 ScienceDirect Selected Article, ChemWeb.com Inorganic, Vol 2 Issue 8, 27 Nov 2003.

28. Laser synthesis of transition metal clusters
JS McIndoe*
 Transition Metal Chemistry, 2003, 28, 122-131 (624 kb Download a pdf file of this article file).
 Invited Literature Highlight.

27. Direct analysis of catalysts immobilised in ionic liquids using electrospray ionisation ion trap mass spectrometry
PJ Dyson*, JS McIndoe* and D Zhao
 Chemical Communications, 2003, 508-509 (331 kb Download a pdf file of this article file).
 Selected as a "Hot Paper".
 Featured in C&EN Concentrates, 24 February 2003.

26. Fragmentation of transition metal carbonyl cluster anions: structural insights from mass spectrometry
CPG Butcher, PJ Dyson, BFG Johnson, T Khimyak and JS McIndoe*
 Chemistry - A European Journal, 2003, 9, 944-950 (244 kb Download a pdf file of this article file).

25. Studies of polyhalide ions in aqueous and non-aqueous solution by electrospray mass spectrometry
JS McIndoe and DG Tuck
 Dalton Transactions, 2003, 244-248 (154 kb Download a pdf file of this article file).

C. Electrospray ionization mass spectrometry
W Henderson and JS McIndoe
a short chapter in Comprehensive Coordination Chemistry 2 (101 kb Download a pdf file of this article file).
Elsevier Publishers, 2003.

B. Metal Carbonyls
JS McIndoe and PJ Dyson
an online article in the Kirk-Othmer Encylopedia of Chemical Technology (306 kb Download a pdf file of this article file).
John Wiley & Sons Publishers, 2003.


2002

24. The preparation and characterisation of monomeric and linked metal carbonyl clusters containing the closo-Si2Co4 pseudo-octahedral core
C Evans, GJ Harfoot, JS McIndoe, CJ McAdam, KM Mackay, BK Nicholson*, BH Robinson and ML Van Tiel
 Journal of the Chemical Society, Dalton Transactions, 2002, 4678-4683 (173 kb Download a pdf file of this article file).

23. On the use of breakdown graphs combined with energy dependent mass spectrometry to provide a complete picture of fragmentation processes
CPG Butcher, PJ Dyson, BFG Johnson, JS McIndoe*, PRR Langridge-Smith and C Whyte
 Rapid Communications in Mass Spectrometry, 2002, 16, 1595-1598 (146 kb Download a pdf file of this article file).

22. Mass spectrometric identification of singly-charged anionic and cationic sulfur, selenium, tellurium and phosphorus species produced by laser ablation
AK Hearley, BFG Johnson*, JS McIndoe and DG Tuck
 Inorganica Chimica Acta, 2002, 334, 105-112 (313 kb Download a pdf file of this article file).
 Invited paper for the A Wojcicki tribute edition.

21. New complexes with M-Si-O or M-Si-S linkages (M = Fe or Co)
JS McIndoe and BK Nicholson*
 Journal of Organometallic Chemistry, 2002, 648, 237-245 (222 kb Download a pdf file of this article file).

20. Bis[dicarbonyl(cyclopentadienyl)ferrio]mercury(II)
JS McIndoe and BK Nicholson*
 Acta Crystallographica Section E, 2002, E58, m53-m54 (222 kb Download a pdf file of this article file).

19. Collision-induced dissociation and photodetachment of singly and doubly charged anionic polynuclear transition metal carbonyl clusters
CPG Butcher, BFG Johnson, JS McIndoe, X Yang, X-B Wang and L-S Wang*
 Journal of Chemical Physics, 2002, 116, 6560-6566 (310 kb Download a pdf file of this article file).

A. Formaldehyde elimination from methoxylated carbonyl clusters
PJ Dyson, BFG Johnson, JS McIndoe*, PRR Langridge-Smith and D Sambrook
a chapter in Modern Coordination Chemistry - the Legacy of Joseph Chatt (385 kb preprint Download a preprint pdf file of this article file)
RSC Books, 2002.

chatt

2001

18. Mass spectrometric method for the rapid characterisation of transition metal carbonyl cluster reaction mixtures
PJ Dyson*, AK Hearley, BFG Johnson, T Khimyak, JS McIndoe* and PRR Langridge-Smith
 Organometallics, 2001, 20, 3970-3974 (90 kb Download a pdf file of this article file).

17. Combining energy-dependent electrospray ionisation with tandem mass spectrometry for the analysis of inorganic compounds
PJ Dyson, AK Hearley, BFG Johnson, JS McIndoe*, C Whyte and PRR Langridge-Smith
 Rapid Communications in Mass Spectrometry, 2001, 15, 895-897 (122 kb Download a pdf file of this article file).
 Featured on the website spectroscopyNOW.com.

16. Laser desorption ionisation versus electrospray ionisation mass spectrometry: applications in the analysis of cluster anions
PJ Dyson*, AK Hearley, BFG Johnson, JS McIndoe* and PRR Langridge-Smith
 Journal of Cluster Science, 2001, 12, 273-283 (159 kb Download a pdf file of this article file).
 Invited paper for the S Martinengo tribute edition.


2000

BK1.  Transition Metal Carbonyl Cluster Chemistry 
Paul J. Dyson and J. Scott McIndoe
 Part of a series of "Advanced Chemistry Texts"
 Gordon & Breach Publishers (book now sold by CRC Press), 2000.
 More details here.

book1

15. Electrospray mass spectrometric characterisation of bimetallic group 8 - gold clusters
R Bhalla, PJ Dyson*, F Lauterwasser, JS McIndoe
 Gold Bulletin, 2000, 33, 56-59 (269 kb ).
 Invited contribution.

14. Formation of the highly unusual cyclic clusters [HM(CO)4]n (M = Mn, n = 4-9; M = Re, n = 4-6)
PJ Dyson, AK Hearley, BFG Johnson*, JS McIndoe, PRR Langridge-Smith
 Journal of the Chemical Society, Dalton Transactions, 2000, 2521-2525 (244 kb Download a pdf file of this article file).

13. Spectroscopic and mass spectrometric methods for the characterisation of metal clusters
BFG Johnson and JS McIndoe*
 Coordination Chemistry Reviews, 2000, 200-202, 901-932 (395 kb Download a pdf file of this article file).
 Invited review for volume 200.

12. Insights into the elimination of HCHO from the clusters [Mn(CO)m(COOMe)]- (Mn = Ru6C, m = 16; Mn = Rh6, m = 15) provided by electrospray mass spectrometry
PJ Dyson, N Feeder, BFG Johnson, JS McIndoe*, PRR Langridge-Smith
 Journal of the Chemical Society, Dalton Transactions, 2000, 1813-1815 (149 kb Download a pdf file of this article file).
 This issue featured cover art from our paper.

11. Generation of supraclusters and nanoclusters using laser desorption/ionisation mass spectrometry
PJ Dyson*, JE McGrady*, M Reinhold, BFG Johnson, JS McIndoe and PRR Langridge-Smith
 Journal of Cluster Science, 2000, 11, 391-401 (161 kb Download a pdf file of this article file).

10. Applications of laser desorption and electrospray ionisation mass spectrometric techniques at the transition between clusters and colloids
PJ Dyson, BFG Johnson*, JS McIndoe and PRR Langridge-Smith
 Inorganic Chemistry, 2000, 39, 2430-2431 (31 kb Download a pdf file of this article file).

9. Energy-dependent electrospray mass spectrometry (EDESI-MS): applications in transition-metal carbonyl chemistry
PJ Dyson, BFG Johnson, JS McIndoe* and PRR Langridge-Smith
 Rapid Communications in Mass Spectrometry, 2000, 14, 311-313 (38 kb Download a pdf file of this article file).
 Special Issue: Papers Presented at BMSS 1999.


1996-9

8. UV laser desorption/ionisation mass spectrometry of the triruthenium clusters Ru3(CO)12-x(PPh3)x
PJ Dyson*, BFG Johnson*, AK Hearley, JS McIndoe and PRR Langridge-Smith*
 Inorganic Chemistry Communications, 1999, 2, 591-594 (127 kb Download a pdf file of this article file).

7. A study of the gas phase behaviour of [Os6(CO)18] and its high yield synthesis using UV LDI mass spectrometry
WJ Dollard, PJ Dyson*, AT Jackson, BFG Johnson*, JS McIndoe and PRR Langridge-Smith*
 Inorganic Chemistry Communications, 1999, 2, 587-590 (119 kb Download a pdf file of this article file).

6. Reactivity and characterization of transition-metal carbonyl clusters using UV laser desorption mass spectrometry
G Critchley, PJ Dyson*, BFG Johnson*, JS McIndoe, RK O'Reilly and PRR Langridge-Smith*
 Organometallics, 1999, 18, 4090-4097 (100 kb Download a pdf file of this article file).

5. Facile cleavage of Si-Si or Si-Ge bonds in the reactions of disilanes or germylsilanes with cobalt carbonyl
JS McIndoe and BK Nicholson*
 Journal of Organometallic Chemistry, 1999, 577, 181-188 (146 kb Download a pdf file of this article file).

4. The reactions of azide ions with metal carbonyl compounds
JS McIndoe and BK Nicholson*
 Journal of Organometallic Chemistry, 1999, 573, 232-236 (111 kb Download a pdf file of this article file).
 Invited paper for the BFG Johnson tribute edition.

3. Mass spectrometric and structural studies of some platinum-group metal complexes: the crystal and molecular structure of trans-[Ru(NO)Cl3(SbPh3)2]
S Chand, RK Coll* and JS McIndoe
 Polyhedron, 1998, 17, 507-511 (438 kb Download a pdf file of this article file).

2. Electrospray mass spectrometry of metal carbonyl complexes
W Henderson, JS McIndoe, BK Nicholson* and PJ Dyson
 Journal of the Chemical Society, Dalton Transactions, 1998, 519-525 (140 kb Download a pdf file of this article file).
 "Publisher's Choice" (accepted for accelerated publication).

1. Electrospray mass spectrometric analysis of neutral metal carbonyl complexes by derivatisation with alkoxide ion
W Henderson, JS McIndoe, BK Nicholson* and PJ Dyson
 Chemical Communications, 1996, 1183-1184 (216 kb Download a pdf file of this article file).



© JS McIndoe, Department of Chemistry, University of Victoria